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For this installment of Tech Tips Tuesday, we pulled another classic from the archives and gave it a refresh. This simple tutorial demonstrates how to clean a sample cone in a Waters Acquity Triple Quadrupole TQD Mass Spectrometer (MS).

Transcript:

  • Open the source enclosure door by unclipping both spring clips.
  • Close the source isolation valve.
  • Disconnect the PTFE tube from the cone gas assembly.
  • Rotate cone gas assembly 90° and gently remove from ion block assembly.
  • Separate the gas cone, sample cone, and O-ring.
  • Place sample cone and gas cone in methanol water and sonicate for 15 minutes.
  • Once sonication process is completed, put a new O-ring, sample cone and gas cone back together.
  • Insert cone gas assembly in ion block assembly and rotate 90° down.
  • Reconnect PTFE tube to the cone gas assembly tube.
  • Open source isolation valve.
  • Close the source enclosure door and secure with both spring clips.

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